A method of examining a configuration of a sample includes the step of irradiating a terahertz pulsed light, which possesses a wavelength to transmit through the sample, to at least two different portions of the sample, the step of detecting at least two electric field amplitude-time resolved waveforms of the terahertz pulsed light transmitted through the first and second portions of the object to be examined, and the step of examining the configuration of the sample based upon phase information obtained from the electric field amplitude-time resolved waveforms detected.
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1. A method of examining a configuration of a sample having a pre-known refractive index, comprising the steps of;
irradiating a terahertz pulsed light, which possesses a wavelength to transmit through the sample, to at least two different portions of the sample, the at least two different portions having a first portion and a second portion;
detecting each electric field amplitude-time resolved waveform of the terahertz pulsed light transmitted for every part through plural portions of the sample; and
examining the configuration of the sample based upon the pre-known refractive index of the sample and phase information obtained from the electric field amplitude-time resolved waveforms detected.
3. A configuration examination device, comprising:
a laser light source generating a short pulsed laser light;
a light dividing portion dividing the short pulsed laser light into a pump light and a probe light;
a light-delay controlling portion controlling a time delay of the pump light or the probe light both divided by the light dividing portion from the short pulsed laser light;
a terahertz pulsed light generating portion optically pumped by the pump light divided by the light dividing portion and generating a terahertz pulsed light with a wavelength to transmit through a sample having a pre-known refractive index;
a light-irradiating portion irradiating the terahertz pulsed light generated by the terahertz pulsed light generating portion to a portion of the sample;
a moving portion placing the sample thereon and moving the sample, so that the light-irradiating portion irradiates the terahertz pulsed light to another portion of the sample;
a light-receiving portion receiving the terahertz pulsed lights transmitted through the portions of the sample moved by the moving portion;
a detecting portion detecting the electric field amplitude-time resolved waveform of the terahertz pulsed light received by the light-receiving portion with the probe light; and
a configuration judging portion judging the configuration of the sample using the pre-known refractive index thereof and the phase information of the electric field amplitude-time resolved waveform.
2. A method of examining a configuration of a sample according to
4. A configuration examination device according to
5. A configuration examination device according to
6. A configuration examination device according to
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This application is based on and claims priority under 35 U.S.C. § 119 to Japanese Patent Application 2006-276513, filed on Oct. 10, 2006, the entire content of which is incorporated herein by reference.
The present invention generally relates to a method and a device for examining a configuration of an object manufactured by injection molding, compression molding, extrusion molding, or the like. More specifically, the present invention relates to a method and a device for irradiating an electromagnetic wave through a sample and examining a bump and a configuration of the sample by a change of the electromagnetic wave passing through the object.
Resin-made components are frequently employed as components of vehicles, digital products, or the like, in place of metal materials in order to reduce weight and cost. Particularly in vehicle components, various sensors are mounted on the vehicles for a high-function controlling of an engine. Therefore, it is no exaggeration to say that quality of configuration of the resin-made components plays a part for reliability of the vehicle. Further, in digital household electric appliances, tiny resin-made members mechanically play important roles, with a tide of miniaturization and integration. In addition, precision components, made of glass and ceramics, also play important roles in the components of the vehicle and of the digital household appliances. Accordingly, it is important to quantitatively evaluate defects in configuration of such components.
Members made of high polymer materials such as resin material and rubbers, and inorganic materials such as glass and ceramics are manufactured by extrusion molding, injection molding, and by compressive burning, for example. However, the members manufactured may include a stepped portion, a blister, a projection, a roughness, or the like.
Conventionally, such defective portions are detected by irradiating an electromagnetic wave (terahertz wave) with wavelength to pass through an object and then examining a change of transparent intensity of the electromagnetic wave after transmitting through the object. For example, one of such defect detecting method and device is disclosed in Japanese Patent No. 2005-43230A (hereinafter, referred to as reference 1).
The above-described defect detecting device detects a defect of an elongated member (such as a pipe member) with uniform cross section on the basis of a change of transparent intensity of an electromagnetic wave passing through the elongated member. However, the transparent intensity of the electromagnetic wave is influenced by a defect inside of the object and compositional homogeneity of composition of the object, for example. Therefore, greater noise may be generated, and sensitivity and precision for defect detection may be lowered. Further, the transparent intensity is integrated in accordance with a direction where the electromagnetic wave is irradiated. Therefore, measurement of the defect from an irradiated direction may not be obtained. Still further, according to the known method and device, existence or nonexistence of the defect at the uniform cross section of the elongated member is qualitatively evaluated. However, the defect of an object without a pipe-shaped configuration may not be quantitatively evaluated. Accordingly, size and shape as three-dimensional configuration of the defect may not be quantitatively evaluated.
A need thus exists for a method and a device for configuration examination which are not susceptible to the drawback mentioned above.
According to an aspect of the present invention, a method of examining a configuration of a sample includes a step of irradiating a terahertz pulsed light, which possesses a wavelength to transmit through the sample, to at least two different portions of the sample. The at least two different portions has a first portion and a second portion. The method of examining a configuration of the sample further includes a step of detecting each electric field amplitude-time resolved waveform of the terahertz pulsed light transmitted for every part through plurals portions of the sample, and a step of examining the configuration of the sample based upon phase information obtained from the electric field amplitude-time resolved waveforms detected. Further according to another aspect of the present invention, a configuration examination device includes a laser light source, a light dividing portion, a light-delay controlling portion, a terahertz pulsed light generating portion, and a light-irradiating portion. The laser light source generates short pulsed laser light. The light dividing portion divides the short pulsed laser light into a pump light and a probe light. The light-delay controlling portion controls a time delay of the pump light or the probe light both divided by the light dividing portion from the short pulsed laser light. The terahertz pulsed light generating portion is optically pumped by the pump light divided by the light dividing portion and generates the terahertz pulsed light with the wavelength to transmit through the object to be examined. The light-irradiating portion irradiates the terahertz pulsed light generated by the terahertz pulsed light generating portion to a portion of the sample. The configuration examination device further includes a moving portion, a light-receiving portion, a detecting portion, and a configuration judging portion. The sample is placed on the moving portion and is moved thereby. Accordingly, the light-irradiating portion irradiates the terahertz pulsed light to another portion of the sample. The light-receiving portion receives the terahertz pulsed lights transmitted through the portions of the sample moved by the moving portion. The detecting portion detects the electric field amplitude-time resolved waveform of the terahertz pulsed light received by the light-receiving portion with the probe light. The configuration judging portion judges the configuration of the sample with the phase information of the electric field amplitude-time resolved waveform.
The foregoing and additional features and characteristics of the present invention will become more apparent from the following detailed description considered with reference to the accompanying drawings, wherein:
An embodiment of the present invention will be described hereinafter with reference to attached drawings. Components possessing the same general configuration between each drawing will be denoted with the same reference numerals and duplicated explanation will be omitted herein.
The laser light source 1 is represented by a mode-locked fiber laser apparatus, for example. The laser light source 1 generates short pulsed laser light P of which pulse width is between femtoseconds and picoseconds. In addition, a small-sized fiber laser is employed as one of the example of the mode-locked fiber laser apparatus, a small sized-fiber laser which possesses central wavelength in 780 nm (nanometer) zone, an average output power of 20 mW (milliwatt), and a pulse repetition frequency of 50 MHz (megahertz).
The light dividing portion 2 is represented by a beam splitter or a wedged plate, for example. The light dividing portion 2 divides the short pulsed laser light P into pump light Pu and probe light Pr.
The light-delay controlling portion 3 is represented by a device attached to a stage (not illustrated) which moves a corner mirror (not illustrated) in a direction of an arrow R1, i.e., in a direction of an axis X, for example. The light-delay controlling portion 3 scans delay time by controlling a path length of the pump light Pu. Additionally, according to the configuration examination device of this embodiment, the light-delay controlling portion 3 is provided in a light path of the pump light Pu. Alternatively, the light-delay controlling portion 3 may be provided in a light path of the probe light Pr.
The terahertz pulsed light generating portion 4 is represented by a dipole antenna configured by a low temperature-grown GaAs (Gallium Arsenide), an InSb (Indium Antimonide) crystal, or an InAs (Indium Arsenide) semiconductor crystal, for example. The terahertz pulsed light generating portion 4 is optically pumped by the pump light Pu, which is divided by the light dividing portion 2, and generates the terahertz pulsed light S with a wavelength to transmit through a sample 8.
The light-irradiating portion 5 is configured by off-axis parabolic mirrors PM1 and PM2, for example. The light-irradiating portion 5 collimates terahertz pulsed light S generated by the terahertz pulsed light generating portion 4, and then gathers the terahertz pulsed light S to around a surface 81 of two parallel surfaces 81 and 82 of the sample 8 so that a light axis OA is oriented perpendicularly relative to the two surfaces 81 and 82 of the sample 8, i.e., in a direction of an axis Z. For example, when a beam diameter of the terahertz pulsed light S collimated by the off-axis parabolic mirror PM1 is assigned as about 15 mm and the terahertz pulsed light S with the diameter of 15 mm is gathered to the off-axis parabolic mirror PM2 with a focal length of 150 mm, a diameter of a gathered light becomes to 2 mm. Accordingly, a numerical aperture of the light-irradiating portion 5, i.e., a numerical aperture NA1 of terahertz pulsed light S irradiating to the sample 8, is about 0.05.
The moving portion 9 is represented by a stage moving in the direction of the axis X, for example. The moving portion 9 moves the sample 8 in a direction of an arrow R2, i.e., in the direction of the axis X. Accordingly, a position of the sample 8, where the light-irradiating portion 5 irradiates the terahertz pulsed light, is changed from one portion (first portion) to another portion (second portion).
The light-receiving portion 6 is configured by off-axis parabolic mirrors PM3 and PM4, for example. The light-receiving portion 6 collimates transmitted terahertz pulsed light S′, which corresponds to the terahertz pulsed light S after passing through the sample 8. Further, the light-receiving portion 6 gathers the transmitted terahertz pulsed light S′ to the detecting portion 7. A focal length of the off-axis parabolic mirror PM3 is 150 mm and an aperture thereof is 50 mm. Numerical aperture NA2 of the light-receiving portion 6 is about 0.16.
The detecting portion 7 includes a ZnTe (Zinic Telluride) crystal 71 as an electro optic crystal (EO crystal), a Walston prism 72, and a balance detector 73. The detecting portion 7 detects an electric field amplitude-time resolved waveform of the terahertz pulsed light, which is received by the light-receiving portion 6, with the probe light (Pr), which is divided by the dividing means 2. More specifically, the balance detector 73 extracts a polarization-rotational amount of the probe light Pr by means of a differential amplifying mechanism, a polarization-rotational amount which is generated by a complicated refraction induced by the ZnTe crystal 71. Accordingly, a signal inputted from the detecting portion 7 to the configuration judging portion 10 which will be described later, includes the electric field amplitude-time resolved waveform, as illustrated in
The configuration judging portion 10 is represented by a personal computer, for example. The configuration judging portion 10 receives the signal amplified by a lock-in amplifier (not illustrated), and then, judging a configuration of the sample 8 from phase information obtained from the electric field amplitude-time resolved waveform as illustrated in
Next, a theory for examining configuration of an sample 8 with the configuration examination device according to the embodiment will be described hereinafter.
At first, a relationship between delay time difference ΔT1 (delay time difference between T1 and T2 (T2−T1)) and step-height D of the concave portion 80 will be described hereinafter. The relationship between the delay time difference ΔT1 represents one of the phase information of the electric field amplitude-time resolved waveform.
Generally, propagation time of the terahertz pulsed light is obtained by dividing the path length thereof by speed of light C. Additionally, when a refractive index of a propagation medium is assigned as N and a propagation distance is assigned as L, the path length of the terahertz pulsed light is obtained by multiplying N with L (NL). Accordingly, a refractive index of the sample 8 corresponds to the propagation medium N, and the thickness of the sample 8 corresponds to the propagation distance L. Further, the step-height of the concave portion 80 of the sample 8 is assigned as D, as aforementioned. Accordingly, the delay time difference ΔT1 is obtained by an equation (1) described as follows:
ΔT1=D(N−1)/C. (1)
Consequently, when the refractive index N of the sample 8 is already known, the step-height D of the concave portion 80 in the direction of the axis Z is obtained by the equation (1). Further, with reference to
In addition, as illustrated in
Generally, light is refracted when passing a boundary surface with different refractive index. For example, according to the present embodiment, when the sample 8 includes inside thereof a defective portion such as a void (gap), the terahertz pulsed light S may not reach the detecting portion 7 because of lens operation performed by a refractive index difference between the defective portion and non-defective portion or a total reflection caused by a critical angle.
In order to reduce an influence of the lens operation and light scattering occurred by the critical angle and the refraction both which are generated by the sample 8, the numerical aperture NA2 of the light-receiving portion 6 is made greater than the numerical aperture NA1 of the light-irradiating portion 5, as will be described hereinafter.
In addition, the off-axis parabolic mirrors PM3 and PM4 are employed to the light-receiving portion 6. Each of the refracted ray □, the ray Δ passing the light axis, and the ray passing through the outer most light path from among the light paths of terahertz lights (reference lights) is guided from a focus point of the off-axis paraboloid mirror PM3. Therefore, when the three rays □, Δ and are gathered onto the ZnTe crystal 71 (EO crystal) of the detecting portion 7 by means of the off-axis parabolic mirror PM4, the three rays □, Δ and surely reach an identical focus point of the ZnTe crystal 71 (EO crystal) 71 without any phase differences. Accordingly, the configuration of the sample 8 can be examined with high precision.
In a case were surface of the sample 8 is not a flat surface, for example, the terahertz pulsed light S, which passes through the sample 8, is refracted in a direction different from a direction of an original light axis because of its inherent configuration and refractive index. In addition, in a case where the sample 8 includes an extraneous, a defective portion, or a void, etc, of which sizes are almost similar to the wavelength, the terahertz pulsed light S receives a light scattering influence in the direction different from the direction of the original light axis. In such a case, the terahertz pulsed light influenced by the refraction and the scattering may not reach to a detecting portion of a detecting element, i.e., when an electro-optic crystal (EO crystal) is employed for detecting the configuration of the sample 8, the terahertz pulsed light S may not reach a specific portion of the crystal which the probe light Pr (short pulsed laser light) for the detection is illuminated, while when a photoconductive antenna is employed, the terahertz pulsed light S may not reach a gap portion of the photoconductive antenna which the probe light Pr irradiates. However, as described above, according to an arrangement of the present invention, each of light collection optics and collimation of the terahertz pulsed light S, after passing through the sample 8, includes a numerical aperture to receive refraction light and scattered light. Further, with the arrangement of the present invention, each light path length of the terahertz pulsed light refracted and scattered is identical in any route. Accordingly, the scattered and refracted terahertz pulsed light and the terahertz pulsed light passing through the light axis reach the detecting portion of the detecting element concurrently.
As a demonstration experiment of the examination theory, the inventor prepared a sample 8b as shown in
At first, refractive index of the sample 8b was measured by means of the configuration examination device shown in
Generally, resin material includes transmittance bandwidth at terahertz light bandwidth (0.1 THz to 10 THz). However, the transmittance bandwidth is different in accordance with each resin material. The PBT material described above includes the bandwidth with 0.2 THz to 1.4 THz, which is an example where the transmittance bandwidth is comparably narrow. When general resin material is employed as the sample, it is preferable that the transmittance bandwidth be from 0.1 THz to 10 THz.
The complex refractive index changes according to physical property anomalous of the sample 8, such as deterioration of the material, infusion of foreign objects, disorder of tissue, and so on. On the contrary, the physical property anomalous may be detected by the complex refractive index.
Next, as illustrated in
As illustrated above, the phase information of the terahertz pulsed light passing through the sample directly appears on the time resolved waveform of the terahertz pulsed light passing through the sample. Therefore, according to the present invention, the stepped portion and the configuration of the sample can be examined by measuring the time resolved waveform but without processing signals such as deconvolution.
Due to the above described method and device of the present invention, the phase information obtained from the electric field amplitude-time resolved waveform of the terahertz pulsed light S is greatly influenced by a light path of the terahertz pulsed light transmitted through the sample 8. Accordingly, detection precision for detecting the configuration of the sample 8 may be high.
Further, according to the present invention, the phase information is the delay time difference ΔT1 between the time T1 when the terahertz pulsed light S transmits through the first portion of the sample and the time T2 when the terahertz pulsed light S transmits through the second portion of the sample (T2−T1).
As described above, the time difference ΔT1 between the time T1 when the terahertz pulsed light S transmits through the first portion of the sample 8 and the time T2 when the terahertz pulsed light S transmits through the second portion of the sample 8 is greatly influenced by a difference of path lengths between the first portion and the second portion. Accordingly, a difference of configuration measurements (step-heights) between the first portion and the second portion may be detected with high precision.
Further according to the present invention, a numerical aperture NA2 of the light-receiving portion 6 is greater than a numerical aperture NA1 of the light irradiating portion 5.
As described above, the terahertz pulsed light S transmitted through the sample 8 is received by the receiving portion 6 with a large numerical aperture NA2. Accordingly, even when the terahertz pulsed light S is scattered because of a defect inside of the object, for example, it may be possible to efficiently receive the terahertz pulsed light S transmitted through the sample 8.
Further, when the terahertz pulsed light S is irradiated to a stepped portion 80 of the sample 8, a configuration of the stepped portion 80 may be examined by irradiating the terahertz pulsed light S once.
The principles, preferred embodiment and mode of operation of the present invention have been described in the foregoing specification. However, the invention which is intended to be protected is not to be construed as limited to the particular embodiments disclosed. Further, the embodiments described herein are to be regarded as illustrative rather than restrictive. Variations and changes may be made by others, and equivalents employed, without departing from the spirit of the present invention. Accordingly, it is expressly intended that all such variations, changes and equivalents which fall within the spirit and scope of the present invention as defined in the claims, be embraced thereby.
Ohtake, Hideyuki, Sugiura, Toshiharu
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