Solid state folded leaf spring force transducers are fabricated by batch photolithographic and etching techniques from a monocrystalline material, such as silicon. The folded leaf spring structure includes elongated gaps separating adjacent leaf spring leg portions, such elongated gaps being oriented parallel to a crystallographic axis of the monocrystalline material. In a preferred embodiment the monocrystalline material is of diamond cubic type and the leaf spring gaps extend in mutually orthogonal directions parallel to the <011> and <011> crystallographic axes, respectively. In a preferred method of fabricating the spring structure, the structure is etched from a monocrystalline wafer by means of an anisotropic etchant so as to more precisely define angles and dimensions of the resultant spring structure. In one embodiment, the gaps between adjacent leg portions of the spring structure are sealed in a fluid tight manner by means of oxide membranes left intact upon etching of the spring structure. In an accelerometer embodiment, sensing masses of equal weight are affixed to opposite sides of the spring structure for dynamically balancing same.

Patent
   RE31459
Priority
Jan 28 1980
Filed
Jan 28 1980
Issued
Dec 06 1983
Expiry
Dec 06 2000
Assg.orig
Entity
unknown
7
7
EXPIRED
1. In a method for fabricating a solid state force transducer of the type including a leaf spring structure having a plurality of leg portions angularly separated about an axis of maximum compliance and supported so that said leg portions of the leaf spring structure are physically displaced relative to the support structure in response to the application of a force to said leaf spring structure, and including an output sensor means responsive to the displacement of at least one of said leg portions for deriving an output which is a function of the force applied to the transducer, the step of:
forming said leaf spring structure of a monocrystalline material.
54. In a solid state force transducer having an axis of maximum compliance relative to a support:
folded cantilever leaf spring means having a plurality of generally coplanar monolithic leaf spring leg portions for support from the support so that said leg portions of said leaf spring means extended as a cantilever from the support and fold back in a folded region adjacent to each other to the axis of maximum compliance, said leg portions and said folded region being physically displaced relative to the support in response to the application of a force to said leaf spring means to be tranduced and directed along said axis of maximum compliance; and
output sensor means responsive to the displacement of at least one of said leg portions in the direction of maximum compliance for deriving an output which is a function of the force applied to the transducer.
38. In a method for fabricating a solid state force transducer, the step of:
forming a folded cantilever leaf spring transducer structure in a wafer by removing portions of the wafer at a selected location through at least one of the major faces of said wafer to define the folded cantilever spring transducer structure, said folded cantilever spring structure including a folded portion having first and second generally parallel coplanar leaf spring leg portions joined together at a joined first end region thereof and second ends of said leg portions being displaceable one with respect to the other, in responsive to the applied force to be transduced, along an axis of maximum compliance generally orthogonal to the plane of said folded leaf spring leg portions and passing through said second end of said first leg portion, the second end of said second leg portion forming a point of support for said folded cantilever spring portion with said joined region of said leaf spring also being displaceable relative to said point of support in response to the applied force being transduced.
2. The method of claim 1 wherein said leg portions of said monocrystalline leaf spring structure are separated by a slot in said monocrystalline material, and including the step of orienting the longitudinal axis of said slot parallel to a crystallographic axis of said monocrystalline material.
3. The method of claim 1 wherein said monocrystalline material is nonmetallic.
4. The method of claim 1 wherein said monocrystalline material is a semiconductive material.
5. The method of claim 1 including, forming a sensing mass structure on said spring structure.
6. The method of claim 5 wherein said step of forming said sensing mass on said spring structure includes, forming said sensing mass structure with approximately equal mass on opposite sides of the plane of the wide dimension of said leaf spring structure.
7. The method of claim 2 wherein said monocrystalline material is of the diamond cubic type and wherein the longitudinal axis of said slot is oriented parallel to one of the <011> and <011> crystallographic axes of said monocrystalline material.
8. The method of claim 2 wherein said step of forming said spring structure of said monocrystalline material includes, etching said spring structure from a wafer of said monocrystalline material.
9. The method of claim 8 wherein said step of etching includes, etching said spring structure with an anisotropic etchant for the monocrystalline material so that said slot is preferentially etched along a predetermined crystallographic plane.
10. The method of claim 9 wherein the monocrystalline material is silicon.
11. The method of claim 10 including the step of, forming piezoresistive elements in said spring structure.
12. The method of claim 8 including the step of, etching a base support structure from said wafer of monocrystalline material, said base support structure being connected to said etched spring structure by an unetched portion of said wafer for supporting said spring structure therefrom.
13. The method of claim 8 wherein said wafer is of diamond cubic crystal type and wherein said wafer has a major face thereof in the <110> crystallographic plane and wherein the wide dimension of said leaf spring is in the <110> crystallographic plane.
14. The method of claim 8 wherein the step of etching includes, etching an array of said spring structures simultaneously from a single wafer.
15. The method of claim 12 wherein the step of etching of said base support structure includes, etching said spring structure so as to leave said base support structure outside of the periphery of said spring structure.
16. The method of claim 12 including the step of mounting said base support structure to the face of a support plate.
17. The method of claim 13 wherein the spring structure includes a pair of mutually opposed E-shaped folded cantilever leaf spring portions having a plurality of intersecting elongated rectilinear slots defining said spring structure, and wherein some of said slots have their longitudinal axes oriented parallel to the <011> crystallographic axis and other ones of said slots have their longitudinal axes oriented parallel to the <011> crystallographic axis.
18. In a method for fabricating a solid state force transducer, the steps of:
forming a leaf spring structure is a wafer by recessing the leaf spring pattern of a selected location through a first major face of said wafer; and
recessing a second recess at a selected location in registration with said first recessed pattern, through the opposite major face of said wafer and intersecting said second recess with said first recessed pattern to define
said leaf spring structure.
19. In a method for fabricating a solid state force transducer, the steps of:
forming a leaf spring structure in a wafer by recessing a leaf spring pattern at a selected location through a first major face of said wafer;
said recessed leaf spring pattern including a pair of mutually opposed E-shaped leaf spring pattern portions, each E-shaped spring pattern portion including a deflectable central leg portion extending outwardly from a central region of the spring structure and a pair of leg portions on opposite side of and extending outwardly from said central region generally parallel to said central leg portion, said outer leg portions being supported at their inner ends from a portion of the wafer and being interconnected at their outer ends to the outer end of said central leg portion for deflection therewith.
20. The method of claim 19 wherein said step of recessing said spring structure from a wafer of said monocrystalline material includes etching said spring structure from said wafer so as to leave an unetched web portion spanning the space between adjacent leg portions of said spring structure, said web portion being substantially thinner than said leg portions being spanned by said web.
21. In a solid state force transducer:
1eaf spring means having a plurality of leg portions angularly separated about an axis of maximum compliance and supported so that said leg portions of said leaf spring means are physically displaced relative to the support structure in response to the application of a force to said leaf spring means;
output sensor means disposed relative to said leaf spring means so as to be responsive to the displacement of at least one of said leg portions in the direction of maximum compliance for deriving an output which is a function of the force applied to the transducer; and
wherein said leaf spring means is of a monocrystalline material.
22. The apparatus of claim 21 wherein said leg portions of said monocrystalline leaf spring means are separated by a slot in said monocrystalline material, and wherein the longitudinal axis of said slot is oriented parallel to a crystallographic axis of said monocrystalline material.
23. The apparatus of claim 1 wherein said monocrystalline material is nonmetallic.
24. The apparatus of claim 21 wherein said monocrystalline material is a semiconductive material.
25. The apparatus of claim 21 including sensing mass means formed on said leaf spring means.
26. The apparatus of claim 25 wherein said sensing mass means is disposed with approximately equal mass on opposite sides of the plane of the wide dimension of said leaf spring means.
27. The apparatus of claim 22 wherein said monocrystalline material is of the diamond cubic type and wherein the longitudinal axis of said slot is oriented parallel to one of the <011> and <011> crystallographic axes of said monocrystalline material.
28. The apparatus of claim 21 wherein said output sensor means includes piezoresistive means formed in said spring structure.
29. The apparatus of claim 21 including base support structure disposed outside of the periphery of said spring structure for supporting said spring structure therefrom.
30. The apparatus of claim 27 wherein said spring structure includes a pair of mutually opposed E-shaped folded catilever leaf spring portions having a plurality of intersecting elongated rectilinear slots defining said spring structure, and wherein some of said slots have their longitudinal axes oriented parallel to the <011> crystallographic axis and other ones of said slots have their longitudinal axes oriented parallel to the <011>
crystallographic axis. 31. The product of the method of claim 8.
38. 32. The product of the method of claim 9.
39. 33. The product of the method of claim 12.
40. 34. The product of the method of claim 14.
42. 35. The product of the method of claim 19.
46. 36. The product of the method of claim 18. 52.
37. The product of the method of claim 20.
39. The method of claim 38 wherein the step of removing portions of the wafer to define said leaf spring structure includes removing portions of the wafer through both major faces of said wafer to define said folded cantilever leaf spring structure. 40. The method of claim 38 wherein said folded cantilever leaf spring structure includes a pair of mutually opposed E-shaped leaf spring portions, each E-shaped leaf spring portion including a deflectable central leg portion extending from the axis of maximum compliance of the spring and a pair of outer deflectable leg portions disposed on opposite sides of and adjacent said central leg portion and extending generally parallel thereto, said pair of outer leg portions being supported at their inner ends from a portion of the wafer and being joined together at their outer ends to the outer end of said central leg portion and said joined outer ends of said outer leg portions being free to deflect relative to their supported ends with deflection of said central leg portion in response to the applied force to be transduced.
41. The method of claim 38 wherein said step of forming said folded cantilever leaf spring structure in said wafer includes etching said spring structure from said wafer so as to leave an unetched web portion spanning the space between adjacent leg portions of said folded cantilever spring structure, said web portion being substantially thinner than said leg portions.
42. The method of claim 38 wherein said wafer includes a monocrystalline portion and wherein said leg portions of said folded cantilever leaf spring structure are defined by slots in said wafer material, and including the step of orienting the longitudinal axes of said slots parallel to a crystallographic axis of said monocrystalline portion of said wafer.
43. The method of claim 42 wherein said monocrystalline portion of said wafer is of diamond cubic type material.
44. The method of claim 38 wherein said cantilever leaf spring material is composed of a material containing silicon.
45. The method of claim 38 including the step of forming a sensing mass structure on said folded cantilever spring structure.
46. The method of claim 45 wherein said step of forming said sensing mass structure on said folded cantilever spring structure includes, forming said sensing mass structure with approximately equal mass on opposite sides of the plane of said folded cantilever leaf spring structure.
47. The method of claim 42 wherein said monocrystalline portion is of diamond cubic type and wherein the longitudinal axes of said slots are oriented parallel to one of the <011> and <011> crystallographic axes of said monocrystalline portion.
48. The method of claim 42 wherein said step of forming said folded cantilever leaf spring structure includes the step of etching said monocrystalline portion of said wafer with an anisotropic etchant for said material so that said slots are preferentially etched along certain predetermined crystallographic planes.
49. The method of claim 38 including the step of etching a base support structure from said wafer, said base support structure being connected to said cantilever leaf spring structure by an unetched portion of said wafer for supporting said folded cantilever spring structure therefrom at said point of support.
50. In a method of claim 42 wherein said monocrystalline wafer portion is of diamond cubic crystal type and wherein said monocrystalline portion has a major face thereof in the (100) crystallographic plane and wherein the plane of said folded cantilever leaf spring structure is in the (100) crystallographic plane.
51. The method of claim 38 wherein the step of forming a folded cantilever spring structure includes forming an array of said folded cantilever leaf spring structures simultaneously from a single wafer.
52. The method of claim 49 wherein the step of etching said base support structure includes, etching said folded cantilever leaf spring structure so as to leave said base support structure outside of the periphery of said spring structure.
53. The method of claim 49 including the step of, mounting said base support structure to the face of a support plate.
55. The apparatus of claim 54 wherein said leaf spring leg portions are made of a monocrystalline material.
56. The apparatus of claim 54 wherein said monolithic leaf spring leg portions are made of a material containing silicon.
57. The apparatus of claim 55 wherein said adjacent leg portions of said monocrystalline folded leaf spring structure are separated by an elongated slot in said monocrystalline material, and wherein the longitudinal axis of said slot is oriented parallel to a crystallographic axis of said monocrystalline material.
58. The apparatus of claim 54 including sensing mass means formed on said folded cantilever leaf spring structure at the axis of maximum compliance.
59. The apparatus of claim 58 wherein said sensing mass means is disposed with approximately equal amounts on opposite sides of the plane of said folded cantilever leaf spring structure.
60. The apparatus of claim 57 wherein said monocrystalline material is of the diamond cubic type and wherein the longitudinal axis of said slot is oriented parallel to one of the <011> and <011> crystallographic axes of said monocrystalline material.
61. The apparatus of claim 54 wherein said output sensor means includes a piezoresistive means disposed relative to said folded cantilever leaf spring structure for detecting bending of said folded cantilever leaf spring structure in response to the applied force to be transduced. 62. The apparatus of claim 54 including a base support structure disposed outside of the periphery of said folded cantilever leaf spring structure for supporting said spring structure therefrom.
63. The apparatus of claim 54 wherein said folded cantilever leaf spring structure includes a pair of mutually opposed E-shaped folded cantilever leaf spring portions having a plurality of intersecting elongated reclinear slots defining said spring structure.
64. The apparatus of claim 63 wherein said folded cantilever leaf spring structure has leg portions made of a diamond cubic type monocrystalline material and wherein some of said slots have their longitudinal axes oriented parallel to the <011> crystallographic axis and other ones of said slots have their longitudinal axes oriented parallel to the <011> crystallographic axis.

This application is a reissue of Pat. No. 4,071,838, dated Jan. 31, 1978, filed Feb. 9, 1976 as application Ser. No. 656,632. 100) crystallographic plane is preferably formed at the upper and lower major surfaces of the wafer 11. Furthermore, the wafer 11, in the case of the silicon, is preferably doped with an N type dopant such as phosphorus to a resistivity of 6 to 8 ohm centimeters. In the second step of the process, the wafer 11 is oxidized on opposite sides to form oxidized layers 12 and 13, as of 8000 angstroms in thickness. This is conveniently achieved by putting the wafers in a furnace at 1150° C. in the presence of oxygen.

In the next step of the process, the oxide layers 12 and 13 are coated on the top side with a photoresist material and on the bottom side with a protective coating, as of krylon. The photoresist coating is exposed by a conventional photolithographic process to an array of transducer patterns, such as the double E-shaped folded cantilever spring pattern 15 of FIG. 4. Furthermore, each of the individual patterns 15 is separated from the adjacent ones by means of rectangular boundary pattern portion or frame 16. After exposure of the photoresist coating 14, it is developed and then etched out to expose the oxide layer 12. The oxide layer is then etched through the slot pattern 15 formed by the photoresist coating by means of a buffered hydrofluoric acid etchant to define the spring patterns 15 and frame patterns 16 in the oxide coating, thereby exposing the silicon wafer through those patterns.

Next, the silicon wafer 11 is etched with an anisotropic etchant such as 25% by weight of sodium hydroxide in wafer. The spring and frame patterns 15 and 16 were aligned to the <110> on the (100) crystallographic plane of the wafer, as shown in FIG. 3, with the lines of the patterns which are to form spring defining gaps or cuts in the wafer structure, oriented parallel to either the <011> crystallographic axis or the <011> crystallographic axis. The proper orientation relative to the wafer 11 is determined by a chord 19 sliced from each wafer such chord 19 running perpendicular to either the <011> or the <011> crystallographic axis.

The anisotropic etchant etches preferentially along the <111>, <111>, <111> and <111> planes, thus precisely defining the gaps or grooves in the surface of the wafer 11 which are to subsequently define the spring structure of the force transducer. In a typical example of an accelerometer, the anisotropic etch is continued to a depth of approximately 25 microns in the upper surface of the monocrystalline wafer 11. In the anisotropic etching step, the krylon protective coating 17 is also etched from the oxide layer 13 on the bottom of the wafer. In the next step, as shown in FIG. 6, the krylon coating 17 is reestablished on the bottom and then the oxide layer 12 is stripped from the upper surface of the wafer 11 by means of etching in dilute hydrofluoric acid. Next, the krylong coating 17 is stripped from the bottom surface by means of a conventional stripper such as phenol.

In the next step as shown in FIG. 7, the upper surface of the wafer 11 is reoxidized to form layer 21 to a thickness of approximately 1600 angstroms. The oxide layer 21 is then coated with photoresist material and exposed via conventional photolithographic exposure techniques to a pattern of radiation corresponding to a plurality of piezoresistors to be formed in the surface of the resultant spring structure or pattern 15. Typically, the piezoresistors are generally of the pattern shown in FIG. 9.

One set of the piezoresistors are oriented with the longitudinal axes of the piezoresistors extending longitudinally of the spring leg portions of the spring structure in a region thereof of maximum stress, such as near the point of support of one of the inner ends of the outer leg portions. A second set of piezoresistors is also formed in that region with their longitudinal axes aligned perpendicular to the longitudinal axis of the particular leg of the spring so as not to pick up a change in piezoresistance due to stress of the spring structure caused by displacement thereof in response to a force applied to the spring along its axis of sensitivity, ji.e., into the paper in FIG. 4.

These two orientations of piezoresistors are utilized in an electrical bridge circuit so that the difference between the piezoresistance yields a measure of the stress in the spring structure and thus a measure of its displacement in response to a force applied thereto to be measured.

Next, the photoresist layer 22 is developed to expose the oxide layer 21 in accordance with the pattern of the piezoresistors to be formed. Next, the back surface of the wafer is coated with krylon, the photoresist is removed in the exposed piezoresistor pattern to expose the underling oxide layer 21 in accordance with the developed patterns 23. Then the oxide layer 21 is etched through with dilute hydrofluoric acid to expose the underlying monocrystalline silicon wafer 11. Then the wafer is stripped of the krylon and the remaining photoresist.

Next, as shown in FIG. 8, boron is diffused into the silicon wafer 11 through the openings 23 in the oxide layer 21. The boron diffusion is obtained by contacting the surface of the silicon wafer 11 with a boron nitride wafer causing the boron nitride wafer to dissociate and the freed boron to diffuse into the wafer to form the piezoresistor, such piezoresistors having a resistivity of 300 ohms per square. Next, the piezoresistor layer 25 is covered over by regrowing a thin layer of oxide 24 over the piezoresistors, such oxide being obtained by exposing the wafer 11 at elevated temperature to a carrier gas of oxygen and nitrogen.

Next, the wafer 11 is coated on the top surface with a photoresist material and exposed to a pattern of radiation corresponding to contact apertures to be made to the opposite ends of each of the piezoresistors 25, as shown at 26 in FIG. 9. The photoresist material is then developed and removed in the regions through which contact is to be made. Next, the thin layer 24 of oxide is etched by dilute hydrofluoric acid to expose the piezoresistors 25 at the contact regions 26. During the etch step, the back surface of the wafer is protected by a coating of krylon. Next, the photoresist material is stripped and aluminum is evaporated to a thickness of approximately one micron over the front surface of the oxide coated wafer, such aluminum making contact to the piezoresistors 25 through the contact openings 26. Then, a photoresist coating is applied over the aluminum and exposed to a pattern of radiation corresponding to the intraconnect lead pattern to be formed on the wafer. The potoresist material is then developed to expose the aluminum in the desired regions and then the aluminum is etched with phosphoric acid. Next the wafer is placed into an oven at 500°C to alloy the aluminum contacts into the piezoresistor regions 25.

Referring now to FIG. 10, next, the bottom side of the wafer 11 is coated with a photoresist material 31 and exposed to a pattern of radiation corresponding to a base support structure which is to surround each of the spring structures. The base support structure is shown in FIG. 13. The photoresist material 31 is then developed and removed in the regions which are to be etched. The top side of the wafer 11 is then coated with krylon and the oxide layer 13 on the bottom side is etched through by means of dilute hydrofluoric acid to define the base structure.

Next, as shown in FIG. 11, the bottom surface of the wafer 11 is coated with a first layer of chromium 32 to a thickness of approximately 500 angstroms followed by a layer of gold 33 to approximately 8000 angstroms in thickness. Next, the metallized layers are coated with a photoresist, exposed to patterns of radiation corresponding to the base structure. The front side of the wafer 11 is protected by krylon and then the back side is etched with an etchant for the gold and chromium layers.

Next the wafer, as shown in FIG. 12, is exposed to an anisotropic etchant for the silicon, such etching producing a recess in the back side of the wafer which extends inwardly to an intersection with the spring defining pattern of recesses in the front surface of the wafer, to define the spring structure and its base support as shown in FIG. 13. More particularly, the resultant spring structure includes a pair of mutually opposed E-shaped springs 35 and 36 each having a pair of outer leg portions 37 supported at their inner ends from inwardly directed portions of the base support 38. The outer legs 37 are interconnected at their outer ends to the outer end of a central leaf spring portion 39.

In a preferred embodiment, two transverse strengthening members 41 are formed at the outer ends of each of the E-shaped spring portions 35 and 36 by stopping the etching at an intermediate point in the formation of the back recess, coating the strips 41 and 42 with a suitable protective material such as cr and gold and then continuing the etch.

A sensing mass 42 is affixed to both the top and bottom surfaces of the central leg portions 39 of the E-shaped leaf springs 35 and 36, as shown in FIG. 14 and in FIG. 13, to facilitate rendering the composite spring structure responsive to acceleration. In a typical example, the masses 42 comprise two 10 milligram squares of gold affixed as by glue to the inner ends of the central leg portions 39 of the E-springs 35 and 36.

When the etching is complete the individual accelerometer or force transducers are individually etched out of the wafer. The wax is then removed from the front surface of the transducers and they are mounted in a conventional dual in-line integrated circuit package as shown in FIG. 16.

More particularly, a base plate 44 is affixed to the upper surface of the inner ends of the lead frames 45. The transducer 46 is die attached to the upper surface of the mounting plate 44 as by conventional die attach techniques utilizing the gold and chromium coating on the bottom surface of the base support structure of the individual force transducers 46. Wire bonding leads 47 are then wire bonded between the individual conductors of the lead frame structure 45 and the respective connecting pads on the front surface of the transducer 46. The front surface of the transducer 46 is shown in greater detail in FIG. 15.

In a typical example, the resultant transducer 46 has a spring thickness of approximately 25 microns, a length of aproximately 200 mils and a width of 150 mils and is approximately 10 mils thick in the region of the surrounding base support structure.

Referring now to FIG. 17, there is shown an alternative spring pattern consisting of four E-springs 35 located at 90° angles about the central axis of sensitivity 40, which is perpendicular to the paper. The spring structure of FIG. 17 is very rigid in response to forces applied normal to the axis of sensitivity. Thus, there is relatively little cross coupling of forces out of the axis of sensitivity into deflection of the structure along the axis of sensitivity.

Referring now to FIG. 18 there is shown a structure for sealing the spring structure in a fluid tight manner while permitting deflection of the spring structure. More particularly, the silicon dioxide coating 21, which was formed on the top surface of the wafer during the step depicted in FIG. 7, is protected, in the region of the slots, through the various processing steps. In the last etching step, as depicted in FIG. 12 the anisotropic etchant does not attack the silicon dioxide, thereby leaving a thin silicon dioxide web interconnecting adjacent leaf spring portions and bridging the gap therebetween. The silicon dioxide web would ordinarily be permeable to water vapor and thus is coated with a suitable sealant such as a layer of tantalum or gold, or parylene.

The advantages of the present invention include the batch fabrication of transducers of the folded spring type which exhibit improved linearity as contrasted with the prior art diaphragm and cantilever force transducers. An accelerometer of the configuration of FIGS. 13 and 15 has yielded an output signal of 20 volts peak-to-peak when tilted through an angle of 360° relative to the earth's gravitational field. The measured peak-to-peak deviation of the output signal from G sin φ, where φ is the angle of tile relative to the gravitational horizontal and G is the earth's gravitational force, was only 0.1 percent of the peak-to-peak full scale output.

As used herein, monocrystalline is defined to include an epitaxial layer grown upon a monocrystalline substrate even though the expitaxial layer may not comprise only a single crystal.

Block, Barry

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Jan 28 1980Harry E., Aine(assignment on the face of the patent)
Jan 28 1980Barry, Block(assignment on the face of the patent)
Dec 17 1981Diax CorporationAINE, HARRY E RELEASED BY SECURED PARTY SEE DOCUMENT FOR DETAILS 0039380193 pdf
Dec 17 1981Diax CorporationBLOCK, BARRYRELEASED BY SECURED PARTY SEE DOCUMENT FOR DETAILS 0039380193 pdf
Nov 26 1984AINE, HARRY E BLOCK, BARRYFROM JOINT TO SOLE0043400220 pdf
Nov 26 1984BLOCK, BARRYBLOCK, BARRYFROM JOINT TO SOLE0043400220 pdf
Nov 26 1984AINE, HARRY E AINE, HARRY E FROM JOINT TO SOLE0043400220 pdf
Nov 26 1984BLOCK, BARRYAINE, HARRY E FROM JOINT TO SOLE0043400220 pdf
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